Quantitative and Qualitative Elemental Analysis of Different Nickel–Titanium Rotary Instruments by Using Scanning Electron Microscopy and Energy Dispersive Spectroscopy
Abstract
This study was designed to determine if the alloy
composition shares an influence with the geometric
design on the physical behavior of nickel-titanium rotary
endodontic instruments. ProTaper, HERO, and K3
files were selected. After sterilized and cleaning with
alcohol, surface analysis was performed using energy
dispersive spectroscopy. Measurements were performed
on the active part and on the shank. SEM
images of fractured instruments were also obtained and
assessed. All three types of instruments were composed
mainly of Nickel (54.3%, SD 0.8) and Titanium
(45.2%, SD 0.9). SEM images revealed similar aspect
with the presence of Kirkendall voids regularly distributed
in the alloy. The results indicate that the difference
in properties and behavior of these three endodontic
rotary shaping instruments is solely related to the respective
geometric characteristics of the instrument
design. (J Endod 2008;34:53–55)
Hani F. Ounsi, DCD, DESE, MSc, FICD,* Ziad Salameh, DCD, DESP, MSc,† Thakib Al-Shalan, DDS, MSc, PhD,† Marco Ferrari, MD, DDS, PhD,‡ Simone Grandini, DDS, PhD,‡ David H. Pashley, DMD, PhD,§ and Franklin R. Tay, BDSc (Hons), PhD‡§